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Reference Material For Environmental Testing

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The CRM is used for the quality control and calibration of analytical instruments in analysis of Ferrotitanium. It is also used for the evaluation and verification of accuracy of the analytical methods. The CRM can be used for the transfer of measured value.

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Certified Values

Table 1. Certified Values for YSBC 15602-2006 (Mass Fraction %)

Number	Elements	Ti	C	Si	Mn	P	S	Cr
YSBC 15602-2006	Certified Values	70.02	0.057	1.47	0.106	0.0071	0.0047	0.039
YSBC 15602-2006	Uncertainty	0.17	0.003	0.03	0.004	0.0005	0.0006	0.003
Number	Elements	Ni	Mo	V	Cu	Al	Fe
YSBC 15602-2006	Certified Values	0.29	0.028	0.011	0.037	0.30	26.57
YSBC 15602-2006	Uncertainty	0.02	0.003	0.002	0.003	0.02	0.13

Analysis Methods

Table 2. Analysis Methods

Composition	Method
Ti	The Ammonium ferric sulfate titration method
C	The Infrared absorption method
Si	ICP-AES Perchloric acid dehydration gravimetric method The silicomolybdic blue spectrophotometric method The Sulphuric acid dehydration gravimetric method
Mn	Periodate photometric method AAS ICP-AES
P	Molybdobismuthylphosphoric blue spectrophotometric method Molybdenum blue spectrophotometric method Molybdenum blue photometry for extraction by butyl acetate Extraction of Molybdenum Blue from N-Butyl and Alcohol-Third Chloromethane ICP-AES
S	The Infrared absorption method
Cr	ICP-AES AAS Diphenyl carbon acyl dihydrazide photometry
Ni	ICP-AES AAS Budione oxime photometry
Mo	Rhodanate-butyl acetate extraction photometryd ICP-AES
V	Tantalum reagent extraction spectrophotometric method ICP-AES
Cu	ICP-AES AAS The DDTC photometric method
Al	ICP-AES EDTA titrimetric method The chrome azurol S photometric method
Fe	ICP-AES Dichromate titration method

Homogeneity Test and Stability Inspection

Expiration of certification: The certification of this CRM is valid until January 1, 2026.

Table 3. Methods for homogeneity testing

Composition	Analysis methods	Minimum sample (g)
Ti	The Ammonium ferric sulfate titration method	0.2
C、S	The Infrared absorption method	0.2
Mn、P、Cr、Ni、Mo、V、Cu、Al	ICP-AES	0.1
Si	Perchloric acid dehydration gravimetric method	0.5
Fe	Dichromate titration method	0.2

Packing and Storage

The certified reference material is packed in glass bottles with plastic covers. The net weight is 50g each. It is suggested to keep dryness when stored.

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